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1 article(s) from Petersen, James V.

Evaluation of a commercial packed bed flow hydrogenator for reaction screening, optimization, and synthesis

Marian C. Bryan,
David Wernick,
Christopher D. Hein,
James V. Petersen,
John W. Eschelbach and
Elizabeth M. Doherty

Beilstein J. Org. Chem. 2011, 7, 1141–1149, doi:10.3762/bjoc.7.132

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Scheme 1: Reduction of 4-(4-azidopiperidin-1-yl)benzonitrile on the H-Cube^®.

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Figure 1: SAH³ schematic with injector port and UV detector. Components: (A) pump; (B) six-position manual in...

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Figure 2: Variation in UV absorbance during the reduction of styrene to ethylbenzene, in the controlled mode ...

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Figure 3: Box plot of data showing the percent conversion of styrene to ethylbenzene as a function of pressur...

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Figure 4: Conversion of styrene to ethylbenzene over 20 reactions in sequence through a single 30 mm 10% Pd/C...

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Figure 5: Cartridge-to-cartridge variability of the substrate conversion based on the reduction of styrene to...

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Figure 6: Conversion of styrene to ethylbenzene in a sequence of reactions alternating between 10% Pd/C and q...

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Figure 7: Leached catalyst from 30 mm 10% Pd/C CatCart^®. First 10 mL wash aliquot (A) compared to second 10 m...

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Published 22 Aug 2011

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